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This paper focuses on the synthesis of thermally stable mesostructure zirconium oxide with a surfactant templating technique. It was shown that the suitable molar ratio of the surfactant to zirconium as well as the suitable temperature of the hydrothermal treatment are of great importance in the synthesis of high quality porous zirconium oxide material. Besides, under the suitable concentration treatment, the phosphoric acid can greatly enhance the thermal stability of the porous material. Photo
